ChemicalBook CAS DataBase List 5-PHENYL-FURAN-2-CARBONYL CHLORIDE

5-PHENYL-FURAN-2-CARBONYL CHLORIDE synthesis

8synthesis methods

Product Name:5-PHENYL-FURAN-2-CARBONYL CHLORIDE
CAS Number:57489-93-7
Molecular formula:C11H7ClO2
Molecular Weight:206.63

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Yield:57489-93-7 100%

Reaction Conditions:

with thionyl chloride in toluene at 70; for 4 h;Product distribution / selectivity;

Steps:

1b

Example lb: 5-phenylfuran-2-carbonyl chloride5-phenylfuran-2-carboxylic acid (15.00 g, 79.71 mmol) was suspended in thionyl chloride (30 mL) and heated at 70°C for 4h. The reaction mixture was dried under vacuum at 60°C to give a light green solid in quantitative yield. This material was used in the next step without further purification.

References:

WO2011/159781,2011,A2 Location in patent:Page/Page column 55

52938-97-3
84 suppliers
$45.00/10mg