5-(thiophen-2-yl)pyridine-3-carboxamide synthesis
- Product Name:5-(thiophen-2-yl)pyridine-3-carboxamide
- CAS Number:1265919-10-5
- Molecular formula:C10H8N2OS
- Molecular Weight:204.25
6165-68-0
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Yield:1265919-10-5 83%
Reaction Conditions:
with 1-(2,6-diisopropylphenyl)-3-(2-oxo-2-(2,4,6-tri-tert-butylphenylamino)ethyl)-1H-imidazol-3-ium bromide;palladium diacetate;potassium carbonate in dichloromethane;water;N,N-dimethyl-formamide at 100; for 5 h;Reflux;Suzuki coupling;
References:
Kumar, Manian Rajesh;Park, Kyungho;Lee, Sunwoo [Advanced Synthesis and Catalysis,2010,vol. 352,# 18,p. 3255 - 3266] Location in patent:supporting information; experimental part