N,N',N''-TRI-P-TOSYLDIETHYLENETRIAMINE, DISODIUM SALT synthesis
- Product Name:N,N',N''-TRI-P-TOSYLDIETHYLENETRIAMINE, DISODIUM SALT
- CAS Number:52601-80-6
- Molecular formula:C25H29N3Na2O6S3
- Molecular Weight:609.69
56187-04-3
96 suppliers
$6.00/250mg
52601-80-6
11 suppliers
$117.00/25g
Yield:52601-80-6 100%
Reaction Conditions:
with sodium formate in methanol;ethanol at 50 - 90; for 2 h;
Steps:
The first product (14.14 g, 25 mmol) was dissolved in ethanol in a 250 ml round bottom flask.(200 ml) and heated to 50 ° C to completely dissolve the first product.After adding 10 ml of 5.4 M sodium formate [MeOH], the solution was warmed to 90 ° C.It was refluxed for another 2 hours. The solution was concentrated and concentrated under reduced pressure at 55 ° C.Add 30 ml of methanol and concentrate to dryness at 45 ° C under reduced pressure.30 ml of methanol was added again, concentrated and concentrated under reduced pressure at 45 ° C, and vacuumed overnight.A second product of white solid (Na2Ts3DET) (15.2 g, 100%) was obtained.
References:
TWI654182,2019,B Location in patent:Paragraph 0043
98-59-9
589 suppliers
$9.00/5g
52601-80-6
11 suppliers
$117.00/25g