ChemicalBook CAS DataBase List TrifluoroMethanesulfonic Acid 7-Methoxy-2,2-diMethyl-4-oxo-4H-1,3-benzodioxin-5-yl Ester

TrifluoroMethanesulfonic Acid 7-Methoxy-2,2-diMethyl-4-oxo-4H-1,3-benzodioxin-5-yl Ester synthesis

7synthesis methods

Product Name:TrifluoroMethanesulfonic Acid 7-Methoxy-2,2-diMethyl-4-oxo-4H-1,3-benzodioxin-5-yl Ester
CAS Number:532394-17-5
Molecular formula:C12H11F3O7S
Molecular Weight:356.27

358-23-6 Synthesis

358-23-6
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532394-23-3 Synthesis

5-Hydroxy-7-Methoxy-2,2-diMethyl-4H-1,3-benzodioxin-4-one

532394-23-3
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TrifluoroMethanesulfonic Acid 7-Methoxy-2,2-diMethyl-4-oxo-4H-1,3-benzodioxin-5-yl Ester

532394-17-5
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Yield:532394-17-5 96%

Reaction Conditions:

with pyridine at 0; for 1.5 h;Inert atmosphere;Stille Cross Coupling;

References:

Bolte, Benoit;Basutto, Jose A.;Bryan, Christopher S.;Garson, Mary J.;Banwell, Martin G.;Ward, Jas S. [Journal of Organic Chemistry,2015,vol. 80,# 1,p. 460 - 470]