N-tert-Butyloxycarbonyl Glutathione DiMethyl Diester Disulfide DiMer synthesis

2synthesis methods

Product Name:N-tert-Butyloxycarbonyl Glutathione DiMethyl Diester Disulfide DiMer
CAS Number:566172-19-8
Molecular formula:C34H56N6O16S2
Molecular Weight:868.97

24424-99-5 Synthesis

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Glycine, L-γ-glutamyl-L-cysteinyl-, 1,3-dimethyl ester

97451-41-7
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N-tert-Butyloxycarbonyl Glutathione DiMethyl Diester Disulfide DiMer

566172-19-8
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Yield:566172-19-8 1.05 g

Reaction Conditions:

Stage #1: di[²H₃-methylo]glutathionewith iodine;triethylamine in N,N-dimethyl-formamide at 0; for 0.25 h;
Stage #2: di-tert-butyl dicarbonate in N,N-dimethyl-formamide; for 1 h;

References:

Chalker, Justin M.;Wood, Charlotte S. C.;Davis, Benjamin G. [Journal of the American Chemical Society,2009,vol. 131,# 45,p. 16346 - 16347] Location in patent:supporting information; experimental part

27025-41-8 Synthesis

27025-41-8
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References