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2993-20-6

6-(trifluoromethyl)-5H-purin-2-amine synthesis

2synthesis methods
19690-23-4 Synthesis
2-Amino-6-iodopurine

19690-23-4
116 suppliers
$22.10/1g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 63 percent / HCl, H2O / dimethylformamide / 6 h / 60 °C
2: 27 percent / KF, CuI, NMP / dimethylformamide / 24 h / 60 °C
3: 92 percent / Dowex 50 X 8 (H(+)), H2O / methanol / 1 h / Heating

References:

Hocek, Michal;Holy, Antonin [Collection of Czechoslovak Chemical Communications,1999,vol. 64,# 2,p. 229 - 241]