ChemicalBook CAS DataBase List 2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE

2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE synthesis

1synthesis methods

Product Name:2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE
CAS Number:60835-75-8
Molecular formula:C17H24O8
Molecular Weight:356.37

14098-24-9
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$42.00/1g

76-05-1 Synthesis

76-05-1
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$9.00/1g

2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE

60835-75-8
73 suppliers
$28.00/5MG

Yield:60835-75-8 70%

Reaction Conditions:

Stage #1:2,3,5,6,8,9,11,12,14,15-decahydro-1,4,7,10,13,16-benzohexaoxacyclooctadecin;trifluoroacetic acid with hexamethylenetetramine for 24.3333 h;Reflux;Inert atmosphere;Cooling with ice;
Stage #2: with hydrogenchloride for 2.5 h;Inert atmosphere;Cooling with ice;

References:

Shao, Shuai;Thomas, Michael B.;Park, Kyu Hyung;Mahaffey, Zoe;Kim, Dongho;D'Souza, Francis [Chemical Communications,2017,vol. 54,# 1,p. 54 - 57] Location in patent:supporting information

FullText

2,3-(4-CARBOXYBENZO)-1,4,7,10,13,16-HEXAOXACYCLOOCTADEC-2-ENE Related Search:

3-ETHOXY-4-HYDROXYBENZYL ALCOHOL 3,4-Diethoxybenzyl alcohol 18-Crown-6 3-ethoxy-4-hydroxybenzoic acid 4-(2-ETHOXYETHOXY)BENZOIC ACID 4'-FORMYLBENZO-18-CROWN 6-ETHER 3-(2-HYDROXY-ETHOXY)-BENZOIC ACID