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2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1,1-heptanediol synthesis

2synthesis methods
-

Yield:64739-16-8 79%

Reaction Conditions:

with trifluorormethanesulfonic acid;1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dichloromethane at 0 - 40;

References:

Yusubov, Mekhman S.;Soldatova, Natalia S.;Postnikov, Pavel S.;Valiev, Rashid R.;Yoshimura, Akira;Wirth, Thomas;Nemykin, Victor N.;Zhdankin, Viktor V. [Chemical Communications,2019,vol. 55,# 54,p. 7760 - 7763] Location in patent:supporting information