1-[(4,6-Dichloro-1,3,5-triazin-2-yl)amino]-9,10-anthracenedione synthesis
2synthesis methods
- Product Name:1-[(4,6-Dichloro-1,3,5-triazin-2-yl)amino]-9,10-anthracenedione
- CAS Number:6522-75-4
- Molecular formula:C17H8Cl2N4O2
- Molecular Weight:371.18
Yield:6522-75-4 93.9%
Reaction Conditions:
with potassium carbonate in acetone;benzene at 20; pH=5.5 - 6; for 10 h;
Steps:
A A, synthesis of compound (II)
The 1-amino-anthraquinone and of cyanuric chloride is dissolved in acetone, by adding the reaction solution of K2CO3 solution holding pH5.5-6, stir at room temperature the reaction 10 hours, obtain reaction product precipitation, filtration, washed with acetone and petroleum ether, 60 °C the lower vacuum drying.
References:
CN104419221,2016,B Location in patent:Paragraph 0031; 0032
