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ChemicalBook CAS DataBase List de-A,B-25-hydroxycholestan-8β-ol

de-A,B-25-hydroxycholestan-8β-ol synthesis

4synthesis methods
WYRKZEJKGNHQNC-UVSNUMOOSA-N

307953-25-9
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(3-chloroprop-1-ene-1,1-diyl)dibenzene

24626-27-5
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Yield:24626-27-5 96%

Reaction Conditions:

with tetrabutyl ammonium fluoride in tetrahydrofuran at 70;desilylation;

References:

Fall;Vitale;Mourino [Tetrahedron Letters,2000,vol. 41,# 38,p. 7337 - 7340]