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7-Iodo-1-indanone synthesis

4synthesis methods
628732-03-6 Synthesis
1H-Inden-1-one, 7-amino-2,3-dihydro- (9CI)

628732-03-6
69 suppliers
$66.00/100mg

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Yield:628732-02-5 43%

Reaction Conditions:

Stage #1: 7-amino-2,3-dihydro-1H-inden-1-onewith hydrogenchloride;sodium nitrite in water;acetic acid at 0; for 0.0833333 h;
Stage #2: with potassium iodide in water;acetic acid at 60; for 1 h;

References:

Nguyen, Phong;Corpuz, Evelyn;Heidelbaugh, Todd M.;Chow, Ken;Garst, Michael E. [Journal of Organic Chemistry,2003,vol. 68,# 26,p. 10195 - 10198]

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