ChemicalBook CAS DataBase List 7-METHYL-6-MERCAPTOPURINE

7-METHYL-6-MERCAPTOPURINE synthesis

7synthesis methods

Product Name:7-METHYL-6-MERCAPTOPURINE
CAS Number:3324-79-6
Molecular formula:C6H6N4S
Molecular Weight:166.2

5440-17-5 Synthesis

5440-17-5
67 suppliers
$57.00/100mg

3324-79-6
14 suppliers
$315.00/0.1g

Yield:3324-79-6 66%

Reaction Conditions:

with thiourea in ethanol at 100; for 2 h;

Steps:

2 Example 2:

A solution of compound 1c in EtOH was prepared, and to the solution of compound 1c (169 mg, 1.0 mmol) in EtOH (10 mL), commercially available thiourea (114 mg, 1.5 mmol) was added, and the reaction was heated to 100° C. with stirring and refluxing for 2 hours. After the TCL detection reaction was completed, suction filtration was performed, and the precipitate was washed with anhydrous EtOH, and spin-dried to obtain compound 2c, 110 mg (white solid), with a yield of 66%.

References:

CN111333651,2020,A Location in patent:Paragraph 0041-0143