Benzenemethanol, 2-nitro-alpha-(trifluoromethyl)- (9CI) synthesis
- Product Name:Benzenemethanol, 2-nitro-alpha-(trifluoromethyl)- (9CI)
- CAS Number:700362-32-9
- Molecular formula:C8H6F3NO3
- Molecular Weight:221.13
Yield:700362-32-9 99%
Reaction Conditions:
Stage #1: (trifluoromethyl)trimethylsilane;2-nitro-benzaldehydewith potassium carbonate in N,N-dimethyl-formamide at 20; for 4 h;
Stage #2: with water in N,N-dimethyl-formamide; for 4 h;Acidic conditions;
References:
Cheng, Huicheng;Pei, Yu;Leng, Faqiang;Li, Jingya;Liang, Apeng;Zou, Dapeng;Wu, Yangjie;Wu, Yusheng [Tetrahedron Letters,2013,vol. 54,# 33,p. 4483 - 4486]
552-89-6
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700362-32-9
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