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ChemicalBook CAS DataBase List (6E,10E)-7,11,15-Trimethyl-3-methylene-1,6,10,14-hexadecatetrene

(6E,10E)-7,11,15-Trimethyl-3-methylene-1,6,10,14-hexadecatetrene synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 50 percent / p-TsOH*H2O / methanol / 0.25 h / Ambient temperature
2: 90 percent / 2,4-dinitrophenol / toluene / 8 h / 110 °C
3: 1.) p-toluenesulfonylhydrazide, 2.) NaBH3CN / 1.) AcOH, 40 min, 2.) 4 h

References:

Baeckstroem, Peter;Li, Lanna [Tetrahedron,1991,vol. 47,# 32,p. 6533 - 6538]

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