β-D-Glucopyranose, 1,6-anhydro-2,3,4-tris-O-(trimethylsilyl)- synthesis

5synthesis methods

Product Name:β-D-Glucopyranose, 1,6-anhydro-2,3,4-tris-O-(trimethylsilyl)-
CAS Number:7449-14-1
Molecular formula:C15H34O5Si3
Molecular Weight:378.68

2280-44-6
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β-D-Glucopyranose, 1,6-anhydro-2,3,4-tris-O-(trimethylsilyl)-

7449-14-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Microwave irradiation; Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 100 °C / Microwave irradiation; Inert atmosphere
2.2: 0.5 h / 20 °C / Microwave irradiation; Inert atmosphere

References:

Ko, Yen-Chun;Tsai, Cheng-Fang;Wang, Cheng-Chung;Dhurandhare, Vijay M.;Hu, Pu-Ling;Su, Ting-Yang;Lico, Larry S.;Zulueta, Medel Manuel L.;Hung, Shang-Cheng [Journal of the American Chemical Society,2014,vol. 136,# 41,p. 14425 - 14431]