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1H-Isoindole-1,3(2H)-dione, 2-(3-methyl-3-penten-1-yl)- synthesis
- Product Name:1H-Isoindole-1,3(2H)-dione, 2-(3-methyl-3-penten-1-yl)-
- CAS Number:75540-48-6
- Molecular formula:C14H15NO2
- Molecular Weight:229.27
![Ethyl 3-methyl-4-oxopentanoate](/CAS/20210305/GIF/55424-74-3.gif)
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![1H-Isoindole-1,3(2H)-dione, 2-(3-methyl-3-penten-1-yl)-](/CAS/20210305/GIF/75540-48-6.gif)
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / dichloromethane; ethanol / 1 h / 0 - 5 °C
2: pyridine / dichloromethane / 0.5 h / 0 °C
3: tetrabutylammomium bromide / N,N-dimethyl-formamide / 2 h / 20 °C
4: lithium chloride; sodium carbonate / 1-methyl-pyrrolidin-2-one / 100 °C
References:
CN112358403,2021,A
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![Methyl 3-methyl-4-oxopentanoate](/CAS/20150408/GIF/25234-83-7.gif)
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![1H-Isoindole-1,3(2H)-dione, 2-(3-methyl-3-penten-1-yl)-](/CAS/20210305/GIF/75540-48-6.gif)
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![1,4-Pentanediol, 3-methyl-](/CAS/20210305/GIF/26787-63-3.gif)
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![2-Acetylbutyrolactone](/CAS/GIF/517-23-7.gif)
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$5.00/25g
![1H-Isoindole-1,3(2H)-dione, 2-(3-methyl-3-penten-1-yl)-](/CAS/20210305/GIF/75540-48-6.gif)
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