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1H-Indole-1,2-dicarboxylic acid, 5-hydroxy-, 1-(1,1-diMethylethyl) 2-ethyl ester synthesis

3synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
823 suppliers
$13.50/25G

24985-85-1 Synthesis
Ethyl 5-hydroxyindole-2-carboxylate

24985-85-1
129 suppliers
$19.00/100mg

1H-Indole-1,2-dicarboxylic acid, 5-hydroxy-, 1-(1,1-diMethylethyl) 2-ethyl ester

796870-15-0
5 suppliers
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Yield:796870-15-0 98%

Reaction Conditions:

with triethylamine in 1,4-dioxane at 70;

References:

Bautista-Aguilera, Oscar M.;Samadi, Abdelouahid;Chioua, Mourad;Nikolic, Katarina;Filipic, Slavica;Agbaba, Danica;Soriano, Elena;De Andrés, Lucía;Rodríguez-Franco, María Isabel;Alcaro, Stefano;Ramsay, Rona R.;Ortuso, Francesco;Ya?ez, Matilde;Marco-Contelles, José [Journal of Medicinal Chemistry,2014,vol. 57,# 24,p. 10455 - 10463] Location in patent:supporting information