ethyl 4-hydroxy-7-phenoxyisoquinoline-3-carboxylate synthesis
- Product Name:ethyl 4-hydroxy-7-phenoxyisoquinoline-3-carboxylate
- CAS Number:808116-52-1
- Molecular formula:C18H15NO4
- Molecular Weight:309.32
108-95-2
743 suppliers
$14.00/25g
808116-52-1
31 suppliers
inquiry
Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: pyridine; quinoline; copper(II) oxide; potassium carbonate / 28 h / 170 °C / Inert atmosphere
2.1: methanol / 25 - 30 °C
2.2: 10 - 15 °C
3.1: phosphorus tribromide / dichloromethane / -10 - 0 °C
4.1: sodium carbonate / acetonitrile / 55 °C
5.1: trichlorophosphate / N,N-dimethyl-formamide / 6 h / 158 °C
6.1: hydrogenchloride / water; ethanol / Reflux
6.2: 30 - 50 °C
References:
CN115594631,2023,A
3132-99-8
492 suppliers
$5.00/10g
808116-52-1
31 suppliers
inquiry
39515-51-0
410 suppliers
$10.00/5g
808116-52-1
31 suppliers
inquiry
13826-35-2
322 suppliers
$6.00/5g
808116-52-1
31 suppliers
inquiry
53874-66-1
148 suppliers
$14.00/1g
808116-52-1
31 suppliers
inquiry