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ChemicalBook CAS DataBase List Benzoesure, 4-[[6-[(1-oxo-2-propenyl)oxy]hexyl]oxy]-, 4-methoxyphenylester

Benzoesure, 4-[[6-[(1-oxo-2-propenyl)oxy]hexyl]oxy]-, 4-methoxyphenylester synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol; water / 36 h / Reflux
2: N,N-dimethyl-aniline / tetrahydrofuran / 48.5 h / 20 °C / Cooling with ice
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48.5 h / 20 °C / Cooling with ice

References:

Chen, Dongzhong;Cheng, Pin;Fang, Jianglin;Wu, Zhongying;Xu, Tianchi;Zhao, Weiguang [New Journal of Chemistry,2020,vol. 44,# 26,p. 10902 - 10910]