Benzoesure, 4-[[6-[(1-oxo-2-propenyl)oxy]hexyl]oxy]-, 4-methoxyphenylester synthesis
- Product Name:Benzoesure, 4-[[6-[(1-oxo-2-propenyl)oxy]hexyl]oxy]-, 4-methoxyphenylester
- CAS Number:82200-53-1
- Molecular formula:C23H26O6
- Molecular Weight:398.45
99-96-7
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82200-53-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol; water / 36 h / Reflux
2: N,N-dimethyl-aniline / tetrahydrofuran / 48.5 h / 20 °C / Cooling with ice
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48.5 h / 20 °C / Cooling with ice
References:
Chen, Dongzhong;Cheng, Pin;Fang, Jianglin;Wu, Zhongying;Xu, Tianchi;Zhao, Weiguang [New Journal of Chemistry,2020,vol. 44,# 26,p. 10902 - 10910]
150-76-5
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83883-26-5
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$8.00/250mg
82200-53-1
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4286-55-9
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82200-53-1
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83883-25-4
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$79.00/1G
82200-53-1
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