3-aminocyclobutane-1-carboxamide hydrochloride, cis synthesis

8synthesis methods

Product Name:3-aminocyclobutane-1-carboxamide hydrochloride, cis
CAS Number:84182-57-0
Molecular formula:C5H11ClN2O
Molecular Weight:150.61

4934-99-0 Synthesis

Cyclobutanecarboxylic acid, 3-hydroxy-, methyl ester

4934-99-0
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3-aminocyclobutane-1-carboxamide hydrochloride, cis

84182-57-0
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 88 percent / pyridine / 336 h
2: 80 percent / NH₄Br, NH₃ / 144 h / Ambient temperature
3: 59 percent / NaN₃ / methanol; H₂O / 20 h / Heating
4: 81 percent / H₂ / PtO₂ / methanol / 6 h / Ambient temperature

References:

Safanda;Sobotka [Collection of Czechoslovak Chemical Communications,1982,vol. 47,# 9,p. 2440 - 2447]