3-Hydroxymethyl-azepane-1-carboxylic acid tert-butyl ester synthesis
- Product Name:3-Hydroxymethyl-azepane-1-carboxylic acid tert-butyl ester
- CAS Number:876147-43-2
- Molecular formula:C12H23NO3
- Molecular Weight:229.32
61472-23-9
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Yield:876147-43-2 76.6%
Reaction Conditions:
with triethylamine in dichloromethane at 12; for 2 h;
Steps:
1.31.1
To a solution of Compound 1 (250 mg, 2.0 mmol) in DCM (5 mL) was added TEA (0.3 mL) followed by Boc2O (426 mg, 2.0 mmol). The mixture was stirred at 12° C. for 2 h. The mixture was concentrated and perified by fish chromatography to give Compound 2 (350 mg, 76.6%).
References:
US2015/197493,2015,A1 Location in patent:Paragraph 0733; 0734; 0735
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