![](/CAS/20211123/GIF/881673-98-9.gif)
881673-98-9 synthesis
- Product Name:881673-98-9
- CAS Number:881673-98-9
- Molecular formula:C13H12FNO3
- Molecular Weight:249.24
![2-Bromo-2'-fluoroacetophenone](/CAS/GIF/655-15-2.gif)
655-15-2
192 suppliers
$5.00/250mg
![Ethyl cyanoacetate](/CAS/GIF/105-56-6.gif)
105-56-6
431 suppliers
$10.00/5ml
![881673-98-9](/CAS/20211123/GIF/881673-98-9.gif)
881673-98-9
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Yield:881673-98-9 100%
Reaction Conditions:
Stage #1: ethyl 2-cyanoacetatewith potassium carbonate at 40 - 45; for 0.75 h;
Stage #2: 2-bromo-2'-fluoroacetophenone in acetone at 20; for 18 h;
References:
Arikawa, Yasuyoshi;Nishida, Haruyuki;Kurasawa, Osamu;Hasuoka, Atsushi;Hirase, Keizo;Inatomi, Nobuhiro;Hori, Yasunobu;Matsukawa, Jun;Imanishi, Akio;Kondo, Mitsuyo;Tarui, Naoki;Hamada, Teruki;Takagi, Terufumi;Takeuchi, Toshiyuki;Kajino, Masahiro [Journal of Medicinal Chemistry,2012,vol. 55,# 9,p. 4446 - 4456] Location in patent:experimental part
![2-Bromo-2'-fluoroacetophenone](/CAS/GIF/655-15-2.gif)
655-15-2
192 suppliers
$5.00/250mg
![881673-98-9](/CAS/20211123/GIF/881673-98-9.gif)
881673-98-9
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![2'-Fluoroacetophenone](/CAS/GIF/445-27-2.gif)
445-27-2
438 suppliers
$9.00/25g
![881673-98-9](/CAS/20211123/GIF/881673-98-9.gif)
881673-98-9
3 suppliers
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