tert-Butyl 4-(4-cyanobenzylamino)piperidine-1-carboxylate synthesis

4synthesis methods

Product Name:tert-Butyl 4-(4-cyanobenzylamino)piperidine-1-carboxylate
CAS Number:888944-30-7
Molecular formula:C18H25N3O2
Molecular Weight:315.41

13035-19-3
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$9.00/1g

tert-Butyl 4-(4-cyanobenzylamino)piperidine-1-carboxylate

888944-30-7
10 suppliers
$309.00/1g

Yield:-

Steps:

Multi-step reaction with 4 steps
1: toluene / 5.5 h / Inert atmosphere; Reflux
2: toluene / 14.08 h / 0 - 20 °C / Inert atmosphere
3: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / Inert atmosphere
4: magnesium sulfate; sodium tetrahydroborate / ethanol / 22 h / 20 - 70 °C / Inert atmosphere

References:

Seifert, Katrin;Buettner, Anita;Rigol, Stephan;Eilert, Nicole;Giannis, Athanassios;Wandel, Elke [Bioorganic and medicinal chemistry,2012,vol. 20,# 21,p. 6465 - 6481,17]

87120-72-7 Synthesis

87120-72-7
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105-07-7
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888944-30-7
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$309.00/1g

References

1029643-92-2
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888944-30-7
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$309.00/1g

References

1-Piperidinecarboxylic acid, 4-[(phenylmethylene)amino]-, 1,1-dimethylethyl ester

1044183-50-7
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888944-30-7
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$309.00/1g

References