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8H-Indeno[1,2-c]thiophen-8-one synthesis

3synthesis methods
23062-41-1 Synthesis
3-Bromo-4-phenylthiophene

23062-41-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: polyphosphoric acid / 200 °C

References:

Bancerz, Mathew;Huck, Lawrence A.;Leigh, William J.;Mladenova, Gabriela;Najafian, Katayoun;Zeng, Xiaofeng;Lee-Ruff, Edward [Journal of Physical Organic Chemistry,2010,vol. 23,# 12,p. 1202 - 1213]