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ChemicalBook CAS DataBase List 9-Acridanone, 10-ethyl-
2207-41-2

9-Acridanone, 10-ethyl- synthesis

6synthesis methods
-

Yield:2207-41-2 88%

Reaction Conditions:

Stage #1: 10H-acridin-9-onewith sodium hydride in N,N-dimethyl-formamide;mineral oil at 20; for 0.5 h;Inert atmosphere;
Stage #2: ethyl iodide in N,N-dimethyl-formamide;mineral oil at 20; for 13.5 h;Inert atmosphere;

References:

Takeda, Takashi;Akutagawa, Tomoyuki [Chemistry - A European Journal,2016,vol. 22,# 23,p. 7763 - 7770]

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