9-AZABICYCLO[3,3,1]NONYL-3-ENDO-OL synthesis

3synthesis methods

Product Name:9-AZABICYCLO[3,3,1]NONYL-3-ENDO-OL
CAS Number:504-12-1
Molecular formula:C8H15NO
Molecular Weight:141.21

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504-12-1
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Yield:98 % ee

Reaction Conditions:

with cis-RuCl₂[dppb][Me-bima];potassium tert-butylate;hydrogen in butan-1-ol at 25; under 7600.51 Torr; for 17 h;Overall yield = 99 %;Time;Reagent/catalyst;Concentration;Solvent;

Steps:

6 Example 6 Preparation Examples of endo-9-azabicyclo[3.3.1]nonan-3-ol

Example 6
Preparation Examples of endo-9-azabicyclo[3.3.1]nonan-3-ol
A reduction reaction of a 9-azabicyclo[3.3.1]nonan-3-one was conducted using a cis-RuCl₂(dppb)(ammp) or a cis-RuCl₂(Me-bima) under the conditions shown in Table 6.
The results are shown in Table 6.

References:

US2016/200726,2016,A1 Location in patent:Paragraph 0110

70243-51-5 Synthesis

9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, endo-

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504-12-1
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References

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References