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ChemicalBook CAS DataBase List 9-Iodo-o-carborane

9-Iodo-o-carborane synthesis

6synthesis methods
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Yield:17830-03-4 97%

Reaction Conditions:

in neat (no solvent);(under N2); tube charged with B-compound and I2 under vac., cooled to liq. N2 temp., sealed, heated to 115°C for 30 min, maintained for 2.5 h, slowly cooled to room temp.; sublimed at 50°C under reduced pressure; elem. anal.;

References:

Barbera, Gemma;Vaca, Albert;Teixidor, Francesc;Sillanpaeae, Reijo;Kivekaes, Raikko;Vinas, Clara [Inorganic Chemistry,2008,vol. 47,# 16,p. 7309 - 7316]