ChemicalBook CAS DataBase List 4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID synthesis

9synthesis methods

Product Name:4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID
CAS Number:91652-00-5
Molecular formula:C17H22O5
Molecular Weight:306.35

The preparation of 4-([6-(methacryloyloxy)hexyl]oxy)benzenecarboxylic acid is as follows:6-(4-Formylphenoxy)hexyl methacrylate in an amount of 116.14 g, 2100 mL of methanol, an aqueous sodium dihydrogen phosphate solution (obtained by dissolving 43 g of sodium dihydrogen phosphate dihydrate in 570 mL of water) and 73 mL of a 30% hydrogen peroxide solution were added one by one. An aqueous sodium chlorite solution (obtained by dissolving 61.9 g of sodium chlorite with the purity of 80% in 500 mL of water) was added by dropping. After dropping, the reaction liquid was stirred at 45° C. for 3 hours, and the reaction was finished. After slowly cooling the reaction liquid to 20° C., 2250 mL of water was dropped to the reaction liquid, and a solid was precipitated. The solid was collected by filtration, and 72.7 g of 4-((6-(methacryloyloxy)hexyl)oxy)benzoic acid was thus obtained.

2009-83-8 Synthesis

2009-83-8
358 suppliers
$7.00/25g

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
42 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 2 steps
1: NaOH, KI
2: C₅H₅N

References:

Mariam, Yitbarek H.;Pemawansa, Kariyawasam P. W.;Okoh, Fred;Bota, Kofi B. [Molecular Crystals and Liquid Crystals (1969-1991),1986,vol. 141,p. 77 - 96]