D-MYO-INOSITOL 2,4,5-TRISPHOSPHATE, HEXAAMMONIUM SALT synthesis
- Product Name:D-MYO-INOSITOL 2,4,5-TRISPHOSPHATE, HEXAAMMONIUM SALT
- CAS Number:92216-45-0
- Molecular formula:C6H15O15P3
- Molecular Weight:420.1
111408-68-5
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92216-45-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: p-TSA*H2O / tetrahydrofuran / 24 h
1.2: 95 percent / AcOH; water / 1 h / 20 °C
2.1: 30 percent / HCl; water / tetrahydrofuran / 72 h / 80 °C
3.1: 1H-tetrazole / CH2Cl2; acetonitrile / 12 h / 20 °C
3.2: 40 mg / m-CPBA / CH2Cl2; acetonitrile / -40 - 20 °C
4.1: H2 / Pd/C / ethanol; H2O / 12 h / 20 °C
4.2: 15 mg / NaOH; water / 3 h / cooling
References:
Podeschwa, Michael A. L.;Plettenburg, Oliver;Altenbach, Hans-Josef [European Journal of Organic Chemistry,2005,# 14,p. 3101 - 3115]
391201-70-0
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92216-45-0
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inquiry