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D-MYO-INOSITOL 4,5-BIS-PHOSPHATE AMMONIUM SALT synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 1H-tetrazole / CH2Cl2 / 4 h / 20 °C
1.2: 65 percent / m-CPBA / CH2Cl2 / -40 - 20 °C
2.1: 99 percent / NaIO4; RuCl3*3H2O / acetonitrile; H2O / 0.13 h / cooling
3.1: 99 percent / H2 / Pd/C / ethanol; H2O / 12 h / 20 °C

References:

Podeschwa, Michael A. L.;Plettenburg, Oliver;Altenbach, Hans-Josef [European Journal of Organic Chemistry,2005,# 14,p. 3101 - 3115]

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