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3-(4-Bromophenyl)-1-(4-methoxyphenyl)-2-propen-1-one synthesis

4synthesis methods
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Yield:92873-00-2 93%

Reaction Conditions:

Stage #1: 1-(4-methoxylphenyl)-2-propen-1-olwith oxygen;palladium diacetate in N,N-dimethyl-formamide at 90; under 760.051 Torr; for 4 h;Green chemistry;
Stage #2: 4-Bromophenylboronic acidwith 2.9-dimethyl-1,10-phenanthroline in N,N-dimethyl-formamide at 90; for 18 h;Green chemistry;chemoselective reaction;Heck Reaction;

References:

Vellakkaran, Mari;Andappan, Murugaiah M. S.;Nagaiah, Kommu [RSC Advances,2014,vol. 4,# 85,p. 45490 - 45494]