(S)-4-(1-Hydrazinylethyl)benzoic Acid Ethyl Ester Benzenesulfonate synthesis
1synthesis methods
- Product Name:(S)-4-(1-Hydrazinylethyl)benzoic Acid Ethyl Ester Benzenesulfonate
- CAS Number:934495-38-2
- Molecular formula:C11H16N2O2.C6H6O3S
- Molecular Weight:366.432
Yield:934495-38-2 83%
Reaction Conditions:
in ethanol at 60;Inert atmosphere;Large scale reaction;optical yield given as %ee;
References:
Yoshikawap, Naoki;Tan, Lushi;Christopher McWilliams;Ramasamy, Deepa;Sheppard, Ruth [Organic Letters,2010,vol. 12,# 2,p. 276 - 279] Location in patent:supporting information; experimental part