[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile synthesis

1synthesis methods

Product Name:[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile
CAS Number:936250-19-0
Molecular formula:C14H18BNO3
Molecular Weight:259.11

533-58-4 Synthesis

533-58-4
363 suppliers
$6.00/5g

[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile

936250-19-0
23 suppliers
$45.00/25mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium carbonate; 18-crown-6 ether / acetone / 1 h / 55 °C / Microwave irradiation
2: triethylamine; palladium diacetate; CyJohnPhos / 1,4-dioxane / 1.5 h / 100 °C / Inert atmosphere

References:

Manasieva, Leda Ivanova;Maria, Battisti Umberto;Prandi, Adolfo;Brasili, Livio;Franchini, Silvia [Synthesis,2015,vol. 47,# 23,art. no. SS-2015-T0293-OP,p. 3767 - 3775]

[2-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-acetonitrile Related Search:

2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENOL 2-METHOXYPHENYLBORONIC ACID PINACOL ESTER