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Butanoic acid, 4-(dimethylamino)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-, (2S)- synthesis

2synthesis methods
125238-99-5 Synthesis
FMOC-DAB(BOC)-OH

125238-99-5
232 suppliers
$9.00/250mg

Butanoic acid, 4-(dimethylamino)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-, (2S)-

949572-13-8
2 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: camphor-10-sulfonic acid / acetonitrile / 0.03 h / 120 °C / Microwave irradiation; Sealed tube
2: formic acid / 2 h
3: sodium cyanoborohydride / methanol; water; 1,4-dioxane / 0.25 h
4: triethylsilane; trifluoroacetic acid / chloroform / 8 h / 60 °C

References:

Lindahl, Fredrik;Hoang, Huy N.;Fairlie, David P.;Cooper, Matthew A. [Chemical Communications,2015,vol. 51,# 21,p. 4496 - 4498]