8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE synthesis

5synthesis methods

Product Name:8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE
CAS Number:98408-17-4
Molecular formula:C10H12BrClN4O2
Molecular Weight:335.58

58-55-9 Synthesis

58-55-9
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8-BROMO-7-(3-CHLOROPROPYL)-1,3-DIMETHYL-2,3,6,7-TETRAHYDRO-1H-PURINE-2,6-DIONE

98408-17-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium chlorate; hydrogen bromide; acetic acid
2: N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate / acetone

References:

Drabczyńska, Anna;Yuzlenko, Olga;K?se, Meryem;Paskaleva, Minka;Schiedel, Anke C.;Karolak-Wojciechowska, Janina;Handzlik, Jadwiga;Karcz, Tadeusz;Kuder, Kamil;Müller, Christa E.;Kie?-Kononowicz, Katarzyna [European Journal of Medicinal Chemistry,2011,vol. 46,# 9,p. 3590 - 3607]