Acetamide, 2-(methylamino)-N-phenyl- synthesis
- Product Name:Acetamide, 2-(methylamino)-N-phenyl-
- CAS Number:31110-53-9
- Molecular formula:C9H12N2O
- Molecular Weight:164.2
Yield:31110-53-9 100%
Reaction Conditions:
in ethanol at 20; for 24 h;Inert atmosphere;
Steps:
General Procedure 1: Synthesis of N-methyl-phenylacetamides
General procedure: Methylamine in 33% EtOH (55 equiv.) was added to a bromoaniline (1 equiv.). The mixturewas stirred at r.t. overnight and solvent removed in vacuo to give the title compound.
References:
Pilkington, Lisa I.;Haverkate, Natalie A.;Van Rensburg, Michelle;Reynisson, Johannes;Leung, Euphemia;Barker, David [Synlett,2016,vol. 27,# 20,art. no. ST-2016-D0513-L,p. 2811 - 2814] Location in patent:supporting information
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