Benzaldehyde, 3-bromo-2,5-dimethoxy- synthesis
- Product Name:Benzaldehyde, 3-bromo-2,5-dimethoxy-
- CAS Number:68216-65-9
- Molecular formula:C9H9BrO3
- Molecular Weight:245.07
50343-02-7
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Yield:68216-65-9 99.7%
Reaction Conditions:
Stage #1: 3-Bromo-2-hydroxy-5-methoxy-benzaldehydewith potassium carbonate in N,N-dimethyl-formamide; for 0.0833333 h;
Stage #2: dimethyl sulfate in N,N-dimethyl-formamide at 20;
References:
Bedernjak, Alexandre F.;Zaytsev, Andrey V.;Babolat, Michèle;Cellier, Marie;James, Arthur L.;Orenga, Sylvain;Perry, John D.;Groundwater, Paul W.;Anderson, Rosaleen J. [Journal of Medicinal Chemistry,2016,vol. 59,# 10,p. 4476 - 4487] Location in patent:supporting information
50343-02-7
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$28.60/10mg
74-88-4
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68216-65-9
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672-13-9
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$39.00/5g
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