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Benzene, 1-(3-bromo-1-propyn-1-yl)-4-nitro- synthesis

5synthesis methods
-

Yield:61266-34-0 91%

Reaction Conditions:

Stage #1: 3-(4-nitrophenyl)prop-2-yn-1-olwith carbon tetrabromide in dichloromethane at 0; for 0.166667 h;
Stage #2: with triphenylphosphine in dichloromethane at 0 - 20;

References:

Okitsu, Takashi;Sato, Kana;Potewar, Taterao M.;Wada, Akimori [Journal of Organic Chemistry,2011,vol. 76,# 9,p. 3438 - 3449] Location in patent:experimental part