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Benzene, 1-chloro-2-(methoxymethyl)- synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 57 percent / Cl2 / CCl4 / 4.5 h / Ambient temperature
2: 28 percent / potassium t-butoxide / tetrahydrofuran / 16 h / Ambient temperature
3: AgNO3 / CCl4 / 0.5 h

References:

Halton, Brian;Randall, Clifford J.;Gainsford, Graeme J.;Robinson, Ward T. [Australian Journal of Chemistry,1987,vol. 40,# 3,p. 475 - 489]

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