Benzoic acid,4,4'-(dimethylsilylene)bis- synthesis
- Product Name:Benzoic acid,4,4'-(dimethylsilylene)bis-
- CAS Number:17003-01-9
- Molecular formula:C16H16O4Si
- Molecular Weight:300.38
Yield:17003-01-9 91%
Reaction Conditions:
Stage #1: bis(4-bromophenyl)dimethylsilanewith n-butyllithium in tetrahydrofuran at -78; for 2 h;
Stage #2: carbon dioxide at -78; for 13 h;
References:
Yuan, Baoling;Gou, Gaozhang;Fan, Tao;Liu, Mingxian;Ma, Yunsheng;Matsuda, Ryotaro;Li, Liangchun [Angewandte Chemie - International Edition,2022,vol. 61,# 28,art. no. E202204568][Angew. Chem.,2022,vol. 134,# 28] Location in patent:supporting information
2097-02-1
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