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ChemicalBook CAS DataBase List BIS(CHLOROMETHYL)DIMETHYLGERMANE

BIS(CHLOROMETHYL)DIMETHYLGERMANE synthesis

2synthesis methods
-

Yield:21581-91-9 69%

Reaction Conditions:

with methyl magnesium iodide in diethyl ether;(Ar); MeMgI soln. added dropwise to Ge compd., refluxed for 2 h; dioxane added, Mg salt filtered off, distd.; elem. anal.;

References:

Barrau, J.;Rima, G.;Satge, J. [Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,1984,vol. 14,p. 21 - 38]

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