CHLOROMETHYLTRIMETHYLGERMANE synthesis
- Product Name:CHLOROMETHYLTRIMETHYLGERMANE
- CAS Number:5830-55-7
- Molecular formula:C4H11ClGe
- Molecular Weight:167.22
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Yield:-
Reaction Conditions:
in diethyl ether;(N2); dropwise addn. (1 h) of a soln. of methyllithium into the soln. of GeCl3CH2Cl at -70 °C under vigorous stirring; addnl. stirring (1.5 h); then standing the mixt. until room temp. was reached and addnl. stirring for 16 h;; filtration; then distg. the solvent off from the filtrate; vacuum distn.;
References:
Tacke, Reinhold;Becker, Beate [Journal of Organometallic Chemistry,1988,vol. 354,# 2,p. 147 - 153]