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ChemicalBook CAS DataBase List BOC-3-AMINO-2-METHYLBENZOIC ACID

BOC-3-AMINO-2-METHYLBENZOIC ACID synthesis

1synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
823 suppliers
$13.50/25G

1975-50-4 Synthesis
2-Methyl-3-nitrobenzoic acid

1975-50-4
443 suppliers
$20.00/25g

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Yield:143617-89-4 86%

Reaction Conditions:

with hydrogen;palladium on activated charcoal in N,N-dimethyl-formamide; under 2585.7 Torr; for 2.5 h;

References:

Tilley, Jefferson W.;Danho, Waleed;Shiuey, Shian-Jun;Kulesha, Irina;Swistok, Joseph;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 21,p. 3774 - 3783]