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Boc-Dap(Z)-OL synthesis

5synthesis methods
61040-22-0 Synthesis
L-Alanine, N-[(1,1-diMethylethoxy)carbonyl]-3-[[(phenylMethoxy)carbonyl]aMino]-, Methyl ester

61040-22-0
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Yield:721927-81-7 78%

Reaction Conditions:

with sodium tetrahydroborate;lithium bromide in tetrahydrofuran;ethanol at 20;Inert atmosphere;Cooling with ice;

References:

Mitra, Roopa;Ganesh [Chemical Communications,2011,vol. 47,# 4,p. 1198 - 1200] Location in patent:supporting information; experimental part