Boc-(R)-3-aMino-2-(hydroxyMethyl)propanoic acid synthesis
- Product Name:Boc-(R)-3-aMino-2-(hydroxyMethyl)propanoic acid
- CAS Number:1190870-93-9
- Molecular formula:C9H17NO5
- Molecular Weight:219.24
58885-60-2
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine / toluene / 0.25 h / pH 7
1.2: 3407 / 30 h / 20 °C
2.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogen phosphate monohydrate / tert-butyl alcohol; water / 6 h
References:
Boeckman, Robert K.;Biegasiewicz, Kyle F.;Tusch, Douglas J.;Miller, John R. [Journal of Organic Chemistry,2015,vol. 80,# 8,p. 4030 - 4045]