ChemicalBook CAS DataBase List Boron triiodide

Boron triiodide synthesis

4synthesis methods

Product Name:Boron triiodide
CAS Number:13517-10-7
Molecular formula:BI3
Molecular Weight:391.52

Boron triiodide can be synthesized by refluxing lithium borohydride and iodine in hexane, or by reacting alkali metal borohydride with iodine at a suitable temperature.

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7553-56-2 Synthesis

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13517-10-7
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$90.79/1g

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Yield:13517-10-7 45-50

Reaction Conditions:

byproducts: HI, I2; at 200°C, under N2; removing of I2: reaction mixt. dissolved in CS2, addn. of Zn or Hg, filtering, evapn. of solvent, sublimation in vac. twice;

References:

Schumb, W. C.;Gamble, E. L.;Danus, M. B. [Journal of the American Chemical Society,1949,vol. 71,p. 3225 - 3229] [Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: B: SVol.1, 4.6, page 204 - 209]