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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Butyric anhydride

Butyric anhydride synthesis

12synthesis methods
To a cooled flask containing 88 gm (1.0 mole) of η-butyric acid at 10°C is added dropwise 28.0 gm (0.5 mole) of methoxyacetylene over a 1-hr period. After stirring the reaction mixture for 16 hr at 20°C the contents are distilled to afford the following three fractions: (1) b.p. 56°C, η& 1.3628, 23 gm (62%), methyl acetate; (2) b.p. 72-73°C (18 mm Hg), n% 1.3990, 10.0 gm (11%), butyric acid; (3) b.p. 91-92°C (18mmHg), 1.4118, 48.0 gm (61%), butyric anhydride.
Preparation of Butyric Anhydride
107-92-6 Synthesis
Butyric Acid

107-92-6
552 suppliers
$9.00/5g

Butyric anhydride

106-31-0
210 suppliers
$10.00/5g

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Yield:106-31-0 95%

Reaction Conditions:

with N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride;triethylamine in dichloromethane at 20; for 0.5 h;

References:

Cabre-Castellvi, J.;Palomo-Coll, A.;Palomo-Coll, A.L. [Synthesis,1981,# 8,p. 616 - 620]

FullText

123-72-8 Synthesis
Butyraldehyde

123-72-8
405 suppliers
$12.32/25ML

Butyric anhydride

106-31-0
210 suppliers
$10.00/5g

References
156-54-7 Synthesis
Sodium Butyrate

156-54-7
424 suppliers
$5.00/5g

Butyric anhydride

106-31-0
210 suppliers
$10.00/5g

References
123-72-8 Synthesis
Butyraldehyde

123-72-8
405 suppliers
$12.32/25ML

107-92-6 Synthesis
Butyric Acid

107-92-6
552 suppliers
$9.00/5g

Butyric anhydride

106-31-0
210 suppliers
$10.00/5g

References
107-92-6 Synthesis
Butyric Acid

107-92-6
552 suppliers
$9.00/5g

Butyric anhydride

106-31-0
210 suppliers
$10.00/5g

Butyryl chloride

141-75-3
331 suppliers
$12.32/25G

References

Butyric anhydride Related Search:

Trifluoromethanesulfonic anhydride Phthalic anhydride Glutaric anhydride Caronic anhydride Butyric Acid Succinic anhydride CIS-BUTENEDIOIC ANHYDRIDE HEPTANOIC ANHYDRIDE VALERIC ANHYDRIDE STEARIC ANHYDRIDE