chloro(p-chlorophenyl)magnesium synthesis
- Product Name:chloro(p-chlorophenyl)magnesium
- CAS Number:51833-36-4
- Molecular formula:C6H4Cl2Mg
- Molecular Weight:171.307
106-39-8
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Yield:-
Reaction Conditions:
at 20; for 3 h;
Steps:
Various fluoro- and chloro-substituted aryl bromides are readily converted into the corresponding magnesium reagents at room temperature using i-PrMgCl·LiCl. The conversion is completed without 0.5-3h which is in strong contrast with the previous procedure involving i-PrMgCl or i-Pr2Mg (Scheme 2).
References:
EP1582523,2005,A1 Location in patent:Page/Page column 6-7
106-46-7
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51833-36-4
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