ChemicalBook CAS DataBase List Chloromethyl ethyl carbonate

Chloromethyl ethyl carbonate synthesis

3synthesis methods

Product Name:Chloromethyl ethyl carbonate
CAS Number:35179-98-7
Molecular formula:C4H7ClO3
Molecular Weight:138.55

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35179-98-7
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Yield:-

Reaction Conditions:

with triethylamine in ethanol;dichloromethane

Steps:

11 4-Phenyl-4-((4-carbo(ethoxycarbonyloxymethoxy) methylpiperazin-1-yl)carboxamido)piperidine hydrochloric acid salt
Combine chloromethyl chloroformate (19 mL) and ichloromethane (300 mL) and cool in an ice bath. Add dropwise over about i hour, a solution of ethanol (11.7 mL and triethylamine (30.7 mL) in dichloromethane (100 mL). After 3.5 hours, filter and concentrate the filtrate to give a residue. Partition the residue between diethyl ether and water. Separate the organic layer and dry over MgSOA, filter and evaporate in vacuo to give ethyl chloromethyl carbonate.

References:

Hoechst Marion Roussel, Inc. US5977139, 1999, A

64-17-5 Synthesis

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22128-62-7
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35179-98-7
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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35179-98-7
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References

Chloromethyl ethyl carbonate Related Search:

Chloromethyl ethyl ether Dimethyl carbonate Ethylene carbonate 2-Butanone oxime Chloroethylene carbonate ChloroMethyl Methyl Carbonate ChloroMethyl Propyl Carbonate L-Alanine Ethyl L-alaninate hydrochloride Diethyl (hydroxymethyl)phosphonate