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ChemicalBook CAS DataBase List 2-Chlorochrysene

2-Chlorochrysene synthesis

2synthesis methods
174265-12-4 Synthesis
2-Bromo-5-chlorobenzaldehyde

174265-12-4
223 suppliers
$6.00/1g

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: anhydrous sodium carbonate; tetrakis-(triphenylphosphine)-palladium / ethanol; lithium hydroxide monohydrate / 18 h / 40 - 70 °C
2: potassium-t-butoxide / tetrahydrofuran / 2 h / 20 °C
3: methanesulfonic acid / dichloromethane / 4 h / 20 °C

References:

KR101489992,2015,B1